Cytenamide trifluoroacetic acid solvate

Johnston, A., Florence, A. J., Fabianni, F. J. A., Shankland, K. ORCID: https://orcid.org/0000-0001-6566-0155, Bedford, C. T. and Bardin, J. (2008) Cytenamide trifluoroacetic acid solvate. Acta Crystallographica Section E: Structure Reports Online, 64 (7). o1215-o1216. ISSN 1600-5368 doi: 10.1107/S1600536808016577

Abstract/Summary

Cytenamide forms a 1:1 solvate with trifluoroacetic acid (systematic name: 5H-dibenzo[a, d] cycloheptatriene-5-carboxamide trifluoroacetic acid solvate), C16H13NO center dot C2HF3O2. The compound crystallizes with one molecule of cytenamide and one of trifluoroacetic acid in the asymmetric unit; these are linked by O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds to form an R-2(2)(8) motif. The trifluoromethyl group of the solvent molecule displays rotational disorder over two sites, with site-occupancy factors of 0.964 (4) and 0.036 (4).

Item Type	Article
URI	https://reading-clone.eprints-hosting.org/id/eprint/13714
Item Type	Article
Refereed	Yes
Divisions	Life Sciences > School of Chemistry, Food and Pharmacy > School of Pharmacy
Uncontrolled Keywords	PARALLEL CRYSTALLIZATION, PACKING MOTIFS, CARBAMAZEPINE, PATTERNS, 10,11-DIHYDROCARBAMAZEPINE
Publisher	International Union of Crystallography
Download/View statistics	View download statistics for this item